Evaluation of the stability of iron(II) solutions by precise coulometric titration with electrogenerated cerium(IV).

Coulometric Titration with Electrogenerated Tin(II). Titration of Platinum(IV)

Cerimetric Determination of Propranolol in Bulk Drug Form and in Tablets

Two simple, accurate and precise methods are described for the determination of propranolol hydrochloride with cerium(IV) sulphate. The titrimetric method is based on the oxidation of the drug by a known excess amount of cerium(IV) sulphate and back titration of the unconsumed oxidant with ammonium ferrous sulphate. In the spectrophotometric method, the unreacted cerium(IV) sulphate is treated ...

Precise Coulometric Titrations of Potassium Dichromate

This paper reports results of a continuing investigation to evaluate coulometric methods of analysis and to develop highly precise and accurate analytical methods for important materials, based upon this technique. Earlier papers described the coulometric titrations of acids and bases [1] 1 and of halides [2]. The present research is concerned with a typical oxidation-reduction titration, the a...

Ultrasound-assisted micellar extraction of phenolic antioxidants from spices and antioxidant properties of the extracts based on coulometric titration data

Ultrasound-assisted micellar extraction of phenolic antioxidants from spices has been developed for the first time. The effect of the surfactant nature and its concentration on the extraction efficiency has been evaluated. Electrogenerated hexacyanoferrate(III) ions have been used as coulometric titrants owing to their selectivity towards phenolic antioxidants. The best recovery of phenolic ant...

What is the weighing form in gravimetric determination of antimony(III) with oxine?

The gravimetric analysis of antimony(III) with oxine (8-quinolinol, Hox) was studied. The amount of antimony left in filtrate and washing solutions was corrected with the results of atomic absorption spectrometry. The weighing form, which had not been conclusive before the present study, was determined to be SbO(ox)(Hox)2. The result (purity of antimony(II) oxide: 99.84 +/- 0.05% (m/m)) of the ...